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Warton MetalsTitration Kits

Warton supply titration kits for the accurate control of the majority of fluxes.  Titration kits are easy to use within the production environment.

Tit33.jpg (14772 bytes)

 

 

Titration Kit Contents

A) 1 x 250 ml plastic conical flask with screw cap.

B) 1 x 10 ml plastic graduated titration syringe.

C) 1 x 5ml polypropylene sampling syringe.

D) 1 x 20 ml glass dropper bottle containing Phenolphthalein indicator solution.

F) 1 x 250 ml bottle of NaOH, N/10 solution.

1 x 500 ml top up bottle of NaOH, N/10 solution available on request.

 

How to use a Titration Kit supplied by Warton

a) Using the sampling syringe, withdraw 5.0 ml of the flux to be titrated, transfer to the vial.

b) Add one drop of the indicator solution.

c) Using the calibrated syringe, fill in the syringe with the titration solution (NaOH N/10) (ensure no air is trapped within the liquid).

d) Place tip of syringe into vial and slowly transfer contents into the vial. The solution will turn purple, but return to clear on agitation/ swirling of vial.

e) Continue adding titration solution (NaOH N/10) in small increments with agitation after each addition until the solution remains purple, i.e. the endpoint has been attained. Note the amount of titration solution needed to reach this permanent colour change, being careful not to pass the minimum addition needed, as this will give a false reading.

f)  Use the titration control chart below to assess the result obtained to the specified range.

 

Titration Control Chart

Titre

Action

14.0 or less

Attention should be given to flux performance. The flux may need replacing.

14.5-15.5

Desired range, no action required

16.0

Add 75 mls Thinners 1000 / Litre of flux

17.5

Add 130 mls Thinners 1000 / Litre of flux

19.0

Add 210 mls Thinners 1000 / Litre of flux

20.0

Add 270 mls Thinners 1000/ Litre of flux

21.0

Add 320 mls Thinners 1000/Litre of flux

22.5

Add 400 mls Thinners 1000/Litre of flux

25.0

Add 520 mls Thinners 1000/Litre of flux

27.5

Add 630 mls Thinners 1000/Litre of flux

30.0+

Attention should be given to flux performance. The flux may need replacing.

Further Information

To request a datasheet or to ask a representative to contact you,  please click on the INFORMATION REQUEST FORM , E.mail sales@warton-metals.co.uk or phone: +44 (0)1706 218888.

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Warton Metals Limited Grove Mill Commerce Street Haslingden Lancashire BB4 5JT England Telephone: +44 (0)1706 218888 Fax: +44 (0)1706 221188 E.mail: sales@warton-metals.co.uk

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